A simple and rapid preparation of pure cellulose confirmed by monosaccharide compositions, delta C-13, yields and C% | |
Li, Q (Li, Qiang)[ 1,2 ]; Liu, Y (Liu, Yu)[ 1,3 ] | |
2013 | |
发表期刊 | DENDROCHRONOLOGIA |
卷号 | 31期号:4(SI)页码:273-278 |
文章类型 | 期刊论文 |
摘要 | A two-step method to extract pure cellulose from tree rings is presented in this study. The method employs the reagents diglyme (diethylene glycol dimethyl ether), hydrochloric acid and sodium chlorite in a 6-h reaction using ordinary equipment. Through separation of the chemical compositions (monosaccharides) using liquid chromatography, the product of this method is shown to contain only glucose from pure cellulose. In contrast, the chemical composition of the "alpha-cellulose" extract obtained by the traditional Jayme-Wise method is primarily glucose and mannose, which may come from hemicelluloses. These results are also verified by comparing the stable carbon isotope ratio (delta C-13), yields and percentage of carbon (C%) of the product extracted by this method and "alpha-cellulose" for different tree species. The results suggest that this method is simple, rapid and appropriate for processing large numbers of small wood samples to develop tree-ring isotope series for high-resolution paleoclimatic research with softwood trees. |
关键词 | Pure Cellulose Two-step Method Liquid Chromatography 13c Yield C% |
DOI | 10.1016/j.dendro.2012.07.005 |
收录类别 | 其他 |
语种 | 英语 |
引用统计 | |
文献类型 | 期刊论文 |
条目标识符 | http://ir.ieecas.cn/handle/361006/9940 |
专题 | 现代环境研究室 |
通讯作者 | Liu, Y (Liu, Yu)[ 1,3 ] |
作者单位 | 1.State Key Laboratory of Loess and Quaternary Geology, Institute of Earth Environment, Chinese Academy of Sciences, Xi’an 710075, PR China; 2.Graduate School of Environmental Studies, Nagoya University, Nagoya 464-8601, Japan; 3.School of Human Settlements and Civil Engineering, Xi’an Jiaotong University, Xi’an 710049, PR China |
推荐引用方式 GB/T 7714 | Li, Q ,Liu, Y . A simple and rapid preparation of pure cellulose confirmed by monosaccharide compositions, delta C-13, yields and C%[J]. DENDROCHRONOLOGIA,2013,31(4(SI)):273-278. |
APA | Li, Q ,&Liu, Y .(2013).A simple and rapid preparation of pure cellulose confirmed by monosaccharide compositions, delta C-13, yields and C%.DENDROCHRONOLOGIA,31(4(SI)),273-278. |
MLA | Li, Q ,et al."A simple and rapid preparation of pure cellulose confirmed by monosaccharide compositions, delta C-13, yields and C%".DENDROCHRONOLOGIA 31.4(SI)(2013):273-278. |
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